The table of contents on page 2 is very useful as it provides links to the different topics that one can click on to instantly go to the section of interest. The prose and delivery is consistent, and it feels as if all subjects are being covered in depth. I did not find items like these in the book. Compatible with any organic chemistry lab manual or set of experiments, it combines specific instructions for three different kinds of laboratory glassware: miniscale, standard taper microscale, and Williamson microscale. For cleaning glassware, use a waste jar, not a waste beaker. Home Description 2nd Edition Table of Contents Download Web Version Table of Contents _ Powered by Create your own unique website with customizable templates. I did not read everything, but what I looked at was accurate. I found the text easy to read. The organic lab manual provides detailed and comprehensive material of general organic laboratory techniques and instrumentation. This book achieves a level of comprehensiveness that I have not seen in an Organic Chemistry lab techniques book before. His groundbreaking lab text, Operational Organic Chemistry, was first published in 1981, and he has written three additional books for the organic chemistry laboratory. Reviewed by Skip Brenzovich, Assistant Professor, Roanoke College on 6/20/17, This laboratory manual is extremely comprehensive, introducing and explaining all of the major techniques that a student might encounter in an introductory organic chemistry lab. Lots of pictures, some complex ideas can be expressed with just a single picture, thereby making the book easy to understand. This is a comprehensive chemistry laboratory manual, and I think the extensive use of pictures makes it more engaging as a resource for educators. The target audience are undergraduate students in organic chemistry. Book: Organic Chemistry Lab Techniques (Nichols), [ "article:topic-category", "authorname:nicholsl", "Lab Techniques", "showtoc:no", "coverpage:yes", "license:ccbyncnd", "lulu@Organic Chemistry Lab Techniques@Lisa Nichols@Butte College" ], lulu@Organic Chemistry Lab Techniques@Lisa Nichols@Butte College, information contact us atinfo@libretexts.org, status page at https://status.libretexts.org. This book presents both paradigms; the time-tested approach as well as the slightly cruder but much more time efficient method. CHM 375/376: Organic Chemistry Lab: Techniques & Safety. The many accompanying pictures and sketches are incredibly useful visual aids. The theory sections are comprehensive, In fact, now that I am aware of this amazing book I will send an e-copy to all my research students and organic lab TAs because this will help them better understand these techniques they are performing on a daily basis. Many photochemical transformations convert simple molecules into extremely complex products with an ease not approached by the standard synthetic chemistry practiced in the laboratory. The material presented in the text is well written, unbiased, and does not contain any obvious errors or inaccuracies. The rapid and ceaseless changing of the presentation of organic chemistry both theoretical and practicalwarranted an entirely new edition, but this would have entailed a massive task, for which neither Discussion of different types of distillations and extractions were thorough. At the time of this project she had taught chemistry fulltimefor 12 years at Butte Community College (in Oroville,northern California, near C.S.U. The picture step-by-step technique summaries will be great for students who have performed techniques previously but need a reminder. There are a few topics that would enhance the book. Even something as simple as reminding students to keep Pasteur pipettes vertical to minimize dripping is addressed. In a few sections, re-organization of the information may provide a greater clarity for the students. Reviewed by Constance Franklin, Assistant professor, Organic chemistry laboratory coordinator, Virginia Commonwealth University on 3/27/18, This book does an excellent job of covering all of the basic techniques used in an organic chemistry lab. The extensive use of photos of actual glassware and techniques Comprehensiveness degree in chemistry from Cornell College and his M.S. Overall, the book gives an excellent overview of all techniques. This is where this book truly stands out; Leonard, Lygo, and Proctors Advanced Practical Organic Chemistry has long been my go-to reference text, but it suffers from the common pitfall of a traditional text: the pictures are black-and-white. As a long-time industrial chemist, I have seen my own practice change from stringent adherence to literature methods to more of a freestyle approach that accomplishes what is necessary in the minimum amount of time. This book does a fantastic job of separating the subject into its components and then exploring those components in detail. In this resource you will find theory and procedures on the main organic lab techniques (chromatography, crystallization, extraction, distillation) as well as general concepts on how to set up and heat apparatuses. Summaries and concepts could be more concise with additional formatting to break up the text and create more digestible sections to aid student focus. This will also be a formidable resource for students to learn about new techniques that they are about to perform for the first time (e.g. Distillations in Figure 1.3a, Figure 5.2, Figure 5.37, and others show a graduated cylinder as a receiver. The diagrams are not distorted, the charts do not flow over diagrams or photos and the photos are razor sharp. Information on certain laboratory techniques is usually available on the internet. There are a few minor corrections that need to be done, but otherwise it is outstanding, and well-written. This book deals with general information about work in Organic Chemistry Laboratory, viz., The book gives an excellent comprehensive view of the various techniques used in organic chemistry. It is also easier to use when other textbooks, so it would be very useful for returning as well as new students- from introductory to advanced levels. The organization was clear and easy to follow. A wonderful, illustrative and well-written lab manual. The information in the book will remain relevant for years to come. Reviewed by Mark Stocksdale, Professor, Earlham College on 12/13/19, This text is very complete and comprehensive for what it is covering. Chapters and subchapters are clearly defined. I loved the books interface. Having pictures certainly made it very enjoyable. Use features like bookmarks, note taking and highlighting while reading Laboratory Techniques in Organic Chemistry, Fourth Edition. The text tells students to leave wet glassware on paper towels. The accompanying images made the text easy to read and follow. It also makes a point to add in cases where students should seek clarification from the professor, which makes it very versatile. Their book, MICROSCALE AND MACROSCALE TECHNIQUES IN THE ORGANIC LABORATORY (Cengage Learning), includes techniques only, and can be used with a faculty member's own experiments. Graphic Violence ; Graphic Sexual Content ; texts. Otherwise, there were no navigation issues encountered. As an electronic text, the clear headings for each section make finding the right information easy. Home Description 2nd Edition Table of Contents Download Web Version Powered by Create your own unique website with customizable templates. Laboratory text for organic chemistry : a source book of chemical and physical techniques Item Preview remove-circle Share or Embed This Item . 5/5 stars ! read more. Section 1.1D talks about greasing joints, which contaminates products. Even the images used will probably still be relevant 10 to 20 years from now. Only a couple of minor errors found: on page 35, Table 1.2, the boiling point of diethyl ether should be 35 oC (instead of 34 oC), and the autoignition temperature of methanol should be 385 oC (instead of 464 oC). read more. As a lab techniques reference it is absolutely singular; even minor and esoteric techniques are covered in such detail that an undergraduate student would be able to (with appropriate practice, of course) master that technique. Flash chromatography is typical for organic labs today, but we are moving from air pressure to solvent delivery pumps, which use different connections and columns. The structure of the textbook was consistent from section to section and easy to follow. It takes into consideration the restrictions of equipment that may be available at different institutions and, when possible, gives different options to use when one procedure may not be possible due to lack of the required equipment or materials. It is well illustrated with a lot of pictures and explanations. YBHAVUBDYLDH Book Laboratory Techniques in Organic Chemistry Download Kindle LABORATORY TECHNIQUES IN ORGANIC CHEMISTRY I.K. The focus on commonly used equipment and glassware in the organic chemistry teaching lab makes this book very relevant. While any long published work likely has a few grammatical errors or typos, I did not notice any in my reading. Although the topic was technical, it didn't feel like a heavy read. All major types of equipment and there uses are covered in sufficient detail that a student should be able to understand the use prior to actual practice in lab. The procedures and concepts are explained carefully in detail. The outline of the text should make any changes straightforward to incorporate. Students will be better able to complete tasks because the pictures provide a better view of the technique. A great deal of attention has been devoted to an accurate presentation of each technique and its variants. The boiling point of diethyl ether is listed correctly on page 145. Each chapter can easily be assigned as a self contained unit. The author writes in a consistent manner in terms of terminology and language throughout the entire text. Butte College . I agree. The abundance of pictures and drawings accompanying the text will make it easy to follow for students. The images and equipment used were institution-specific but the author tries to make note, when appropriate, about how the piece of equipment available may differ and encourages the students to consult with their instructors. The information is presented in a reasonable order. I needed this book for my Organic Chemistry 1 lab. Home Description 2nd Edition Table of Contents Download Web Version Web Version. Then the manual moves to more advanced topics that may require understanding of the previously covered topics. The Chromatography chapter is particularly good and complete, and again, the pictures included provide an excellent view to go along with the chapter text. The book provides a detailed table of contents with links enabling easy movement within the text. This book, because it is in digital format, isnt limited to cheap-to-print black and white, but instead has full color pictures, and a lot of them. This laboratory manual is extremely comprehensive, introducing and explaining all of the major techniques that a student might encounter in an introductory organic chemistry lab. While there was no real discussion of IR or NMR, those can be highly instrument specific in terms of set up and interface and may need to be treated at a more local level. (Delbert Gleason) DISCLAIMER | DMCA. On page 22, first paragraph, second sentence, "which indicates that no volume has been delivered with the pipette is still full." The organic chemistry lab is an unnecessary source of anxiety and stress for many second-year chemistry students. Either the material could be reorganized or at least a link provided to the later part of the section that explains the theory behind the visualization. Complete text is available online. Its purpose is to introduce students to the colorimetric method as an analytical technique, spectrophotometric analysis, water sample analysis, and quantitative techniques in volumetric analysis. Every time I opened it I had to scroll down to where I had left off rather than clicking on the topic I left off on in a table of contents. Otherwise, I had to scroll through many pages to go where I want. However, all of the techniques should be demonstrated in a hood, not a lab bench. The text is internally consistent in terms of terminology and framework. CHM 375/376: Organic Chemistry Lab: Techniques & Safety. Using infographics and color-coded boxed articles across the entire manual would help to identify similar themes such as safety and methods quickly. The technique summaries provided at the end of the book are very useful refreshers, and I will likely be referring students to it often. The book includes detailed descriptions of all relevant techniques used in intro organic chemistry lab as well as some more advanced techniques. The hyperlinks within the Table of Contents makes navigating the book very easy. All the discussed techniques are very commonly used in undergraduate research and teaching labs. Also on page 29, Figure 1.31, in the figure caption, item d) "Withdrawing inert gas in order to flushing the syringe." This is a work of very high quality. Get Started. 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